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Detailed reference covering all aspects of working in laboratories, including safety, fundamentals of analytical techniques, lab instrumentation, and more
A comprehensive study of analytical chemistry as it pertains to the laboratory analyst and chemist, Analytical Chemistry begins with an introduction to the laboratory environment, including safety, glassware, common apparatuses, and lab basics, and continues on to guide readers through the fundamentals of analytical techniques, such as spectroscopy and chromatography, and introduce examples of laboratory programs, such as Laboratory Information Management Systems (LIMS).
This newly updated and revised Second Edition of Analytical Chemistry offers expanded chapters with new figures and the latest developments in the field.
Included alongside this new edition is an updated companion teaching, reference, and toolkit program called ChemTech. Conveniently available via either app or browser, the ChemTech program contains exercises that highlight and review topics covered in the book and features useful calculators and programs, including solution makers, graphing tools, and more. To aid in reader comprehension, the program also includes an interactive periodic table and chapter summaries.
Written by two highly qualified authors with significant experience in both practice and academia, Analytical Chemistry covers sample topics such as:
- Basic mathematics in the laboratory, including different units, the metric system, significant figures, scientific calculators, and ChemTech conversion tools
- Analytical data treatment, including errors in the laboratory, precision versus accuracy, normal distribution curves, and determining errors in methodology
- Plotting and graphing, including graph construction, curve fitting, graphs of specific equations, least-squares method, and computer-generated curves
- Ultraviolet/visible (UV/Vis) spectroscopy, including wave and particle theory of light, light absorption transitions, the color wheel, and pigments
With complete coverage of the practical aspects of analytical chemistry, Analytical Chemistry prepares students for a rewarding career as a chemist or a laboratory technician. Thanks to ChemTech integration, the book is also a useful and accessible reference for the established chemist or technician already working in the laboratory.
Detailed reference covering all aspects of working in laboratories, including safety, fundamentals of analytical techniques, lab instrumentation, and more
A comprehensive study of analytical chemistry as it pertains to the laboratory analyst and chemist, Analytical Chemistry begins with an introduction to the laboratory environment, including safety, glassware, common apparatuses, and lab basics, and continues on to guide readers through the fundamentals of analytical techniques, such as spectroscopy and chromatography, and introduce examples of laboratory programs, such as Laboratory Information Management Systems (LIMS).
This newly updated and revised Second Edition of Analytical Chemistry offers expanded chapters with new figures and the latest developments in the field.
Included alongside this new edition is an updated companion teaching, reference, and toolkit program called ChemTech. Conveniently available via either app or browser, the ChemTech program contains exercises that highlight and review topics covered in the book and features useful calculators and programs, including solution makers, graphing tools, and more. To aid in reader comprehension, the program also includes an interactive periodic table and chapter summaries.
Written by two highly qualified authors with significant experience in both practice and academia, Analytical Chemistry covers sample topics such as:
- Basic mathematics in the laboratory, including different units, the metric system, significant figures, scientific calculators, and ChemTech conversion tools
- Analytical data treatment, including errors in the laboratory, precision versus accuracy, normal distribution curves, and determining errors in methodology
- Plotting and graphing, including graph construction, curve fitting, graphs of specific equations, least-squares method, and computer-generated curves
- Ultraviolet/visible (UV/Vis) spectroscopy, including wave and particle theory of light, light absorption transitions, the color wheel, and pigments
With complete coverage of the practical aspects of analytical chemistry, Analytical Chemistry prepares students for a rewarding career as a chemist or a laboratory technician. Thanks to ChemTech integration, the book is also a useful and accessible reference for the established chemist or technician already working in the laboratory.
Bryan M. Ham, PhD, has worked in analytical chemistry laboratories for more than 25 years. He is currently working for the Department of Homeland Security at the U.S. Customs and Border Protection Office of Trade Headquarters in Washington D.C.
Aihui MaHam, PhD, is an expert in nano-materials including the synthesis and characterization of chemical and biological nano-sensors. She is currently working for the Department of Homeland Security at the U.S. Customs and Border Protection Office of Trade Headquarters in Washington D.C.
About the Authors xxiii
Preface xxv
Acknowledgments xxvii
About the Companion Website xxviii
1 Chemist and Technician in the Analytical Laboratory 1
1.1 Introduction-The Analytical Chemist and Technician 1
1.2 Today's Laboratory Chemist and Technician 1
1.3 ChemTech-The Chemist and Technician Toolkit Companion 2
1.4 Chapter Layout 2
1.5 Users of ChemTech 6
2 Introduction to the Analytical Laboratory 7
2.1 Introduction to the Laboratory 7
2.2 Laboratory Glassware 7
2.3 Conclusion 18
3 Laboratory Safety 19
3.1 Introduction 19
3.2 Proper Personal Protection and Appropriate Attire 19
3.3 Proper Shoes and Pants 20
3.4 Laboratory Gloves 20
3.5 General Rules to Use Gloves 22
3.6 Safety Data Sheet (SDS) 22
3.7 Emergency Eyewash and Face Wash Stations 24
3.8 Emergency Safety Showers 25
3.9 Fire Extinguishers 25
3.10 Clothing Fire in The Laboratory 26
3.11 Spill Cleanup Kits 26
3.12 Chemicals and Solvents 27
3.13 First Aid Kits 29
3.14 Gasses and Cylinders 29
3.15 Sharps Containers and Broken Glass Boxes 30
3.16 Occupational Safety and Health Administration (OSHA) 30
4 Basic Mathematics in the Laboratory 83
4.1 Introduction to Basic Math 83
4.2 Units and Metric System 83
4.3 Significant Figures 84
4.4 Scientific Calculators 86
4.5 ChemTech Conversion Tool 89
4.6 Chapter Key Concepts 96
4.7 Chapter Problems 96
5 Analytical Data Treatment (Statistics) 97
5.1 Errors in the Laboratory 97
5.2 Expressing Absolute and Relative Errors 98
5.3 Precision 98
5.4 The Normal Distribution Curve 98
5.5 Precision of Experimental Data 100
5.6 Normal Distribution Curve of a Sample 101
5.7 ChemTech Statistical Calculations 102
5.8 Student's Distribution t Test for Confidence Limits 105
5.9 Tests of Significance 111
5.10 Treatment of Data Outliers 112
5.11 Chapter Key Concepts 114
5.12 Chapter Problems 114
6 Plotting and Graphing 116
6.1 Introduction to Graphing 116
6.2 Graph Construction 116
6.3 Rectangular Cartesian Coordinate System 117
6.4 Curve Fitting 117
6.5 Redrawn Graph Example 117
6.6 Graphs of Equations 118
6.7 Least-Squares Method 121
6.8 Computer-Generated Curves 122
6.9 Calculating Concentrations 125
6.10 Nonlinear Curve Fitting 126
6.11 Chapter Key Concepts 130
6.12 Chapter Problems 130
7 Using Microsoft Excel® in the Laboratory 132
7.1 Introduction to Excel® 132
7.2 Opening Excel in ChemTech 132
7.3 The Excel Spreadsheet 132
7.4 Graphing in Excel 134
7.5 Complex Charting in Excel 137
7.6 Statistical Analysis using Excel 139
8 Making Laboratory Solutions 151
8.1 Introduction 151
8.2 Laboratory Reagent Fundamentals 151
8.3 The Periodic Table 151
8.4 Calculating Formula Weights 152
8.5 Calculating The Mole 152
8.6 Molecular Weight Calculator 152
8.7 Expressing Concentration 153
8.8 The Parts PER (PP) Notation 157
8.9 Computer-Based Solution Calculations 157
8.10 Reactions in Solution 161
8.11 Chapter Key Concepts 161
8.12 Chapter Problems 162
9 Acid-Base Theory and Buffer Solutions 163
9.1 Introduction 163
9.2 Acids and Bases in Everyday Life 163
9.3 The Litmus Test 163
9.4 Early Acid-Base Descriptions 164
9.5 Br¿nsted-Lowry Definition 164
9.6 The Equilibrium Constant 165
9.7 The Acid Ionization Constant 165
9.8 Calculating the Hydrogen Ion Concentration 165
9.9 The Base Ionization Constant 167
9.10 Ion Product for Water 168
9.11 The Solubility Product Constant (K SP) 168
9.12 The pH of a Solution 170
9.13 Measuring the pH 171
9.14 Buffered Solutions-Description and Preparing 172
9.15 ChemTech Buffer Solution Calculator 174
9.16 Chapter Key Concepts 175
9.17 Chapter Problems 175
10 Titration-A Volumetric Method of Analysis 178
10.1 Introduction 178
10.2 Reacting Ratios 178
10.3 The Equivalence Point 179
10.4 Useful Relationships for Calculations 179
10.5 Deriving the Titration Equation 179
10.6 Titrations in ChemTech 180
10.7 Acid/Base Titration Endpoint (Equivalence Point) 181
10.8 Acid/Base Titration Midpoint 182
10.9 Acid/Base Titration Indicators 182
10.10 Titrations Using Normal Solutions 184
10.11 Polyprotic Acid Titration 184
10.12 ChemTech Calculation of Normal Titrations 185
10.13 Performing a Titration 185
10.14 Primary Standards 186
10.15 Standardization of Sodium Hydroxide 187
10.16 Conductometric Titrations (Nonaqueous Solutions) 189
10.17 Precipitation Titration (MOHR Method for Halides) 190
10.18 Complex Formation with Back Titration (Volhard Method for Anions) 191
10.19 Chapter Key Concepts 196
10.20 Chapter Problems 197
11 Oxidation-Reduction (Redox) Reactions 199
11.1 Introduction 199
11.2 Oxidation and Reduction 199
11.3 The Volt 200
11.4 The Electrochemical Cell 200
11.5 Redox Reaction Conventions 200
11.6 The Nernst Equation 202
11.7 Determining Redox Titration Endpoints 203
11.8 Potentiometric Titrations 204
11.9 Visual Indicators used in Redox Titrations 206
11.10 Pretitration Oxidation-Reduction 207
11.11 Ion-Selective Electrodes 207
11.12 Chapter Key Concepts 207
11.13 Chapter Problems 209
12 Laboratory Information Management System (LIMS) 211
12.1 Introduction 211
12.2 Lims Main Menu 211
12.3 Logging in Samples 213
12.4 Entering Test Results 213
12.5 Add or Delete Tests 214
12.6 Calculations and Curves 214
12.7 Search Wizards 215
12.8 Approving Samples 217
12.9 Printing Sample Reports 217
13 Ultraviolet and Visible (UV/VIS) Spectroscopy 227
13.1 Introduction to Spectroscopy in the Analytical Laboratory 227
13.2 The Electromagnetic Spectrum 227
13.3 Ultraviolet/Visible (UV/VIS) Spectroscopy 227
13.4 UV/Visible Spectrophotometers 236
13.5 Special Topic (Example)-Spectrophotometric Study of Dye Compounds 237
13.6 Chapter Key Concepts 240
13.7 Chapter Problems 242
14 Fluorescence Optical Emission Spectroscopy 244
14.1 Introduction to Fluorescence 244
14.2 Fluorescence and Phosphorescence Theory 245
14.3 Phosphorescence 246
14.4 Excitation and Emission Spectra 247
14.5 Rate Constants 247
14.6 Quantum Yield Rate Constants 248
14.7 Decay Lifetimes 248
14.8 Factors Affecting Fluorescence 249
14.9 Quantitative Analysis and Beer-Lambert Law 252
14.10 Quenching of Fluorescence 253
14.11 Fluorometric Instrumentation 253
14.12 Special Topic-Fluorescence Study of Dye-A007 Complexes 259
14.13 Chapter Key Concepts 261
14.14 Chapter Problems 262
15 Fourier Transform Infrared (FTIR) Spectroscopy 264
15.1 Introduction 264
15.2 Basic IR Instrument Design 264
15.3 The Infrared Spectrum and Molecular Assignment 266
15.4 FTIR Table Band Assignments 267
15.5 FTIR Spectrum Example I 273
15.6 FTIR Spectrum Example II 273
15.7 FTIR Inorganic Compound Analysis 274
15.8 Chapter Key Concepts 274
15.9 Chapter Problems 276
16 Nuclear Magnetic Resonance (NMR) Spectroscopy 280
16.1 Introduction 280
16.2 Frequency and Magnetic Field Strength 280
16.3 Continuous-Wave NMR 281
16.4 The NMR Sample Probe 282
16.5 Pulsed-Field Fourier Transform NMR 282
16.6 Proton NMR Spectra Environmental Effects 284
16.7 Carbon-13 NMR 286
16.8 Special Topic-NMR Characterization of Cholesteryl Phosphate 290
16.9 Chapter Key Concepts 295
16.10 Chapter Problems 296
References 297
17 Atomic Absorption Spectroscopy (AAS) 298
17.1 Introduction 298
17.2 Atomic Absorption and Emission Process 298
17.3 Atomic Absorption and Emission Source 299
17.4 Source Gases and Flames 299
17.5 Block Diagram of AAS Instrumentation 299
17.6 The Light Source 301
17.7 Interferences in AAS 302
17.8 Electrothermal Atomization-Graphite Furnace 302
17.9 Instrumentation 303
17.10 Flame Atomic Absorption Analytical Methods 304
18 Atomic Emission Spectroscopy 306
18.1 Introduction 306
18.2 Elements in Periodic Table 306
18.3 The Plasma Torch 306
18.4 Sample Types 307
18.5 Sample Introduction 308
18.6 ICP-OES Instrumentation 308
18.7 ICP-OES Environmental Application Example 313
19 Atomic Mass Spectrometry 328
19.1 Introduction 328
19.2 Low-Resolution ICP-MS 328
19.3 High-Resolution ICP-MS 331
20 X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD) 336
20.1 X-Ray Fluorescence Introduction 336
20.2 X-Ray Fluorescence Theory 336
20.3 Energy-Dispersive X-Ray Fluorescence (EDXRF) 337
20.4 Wavelength Dispersive X-Ray Fluorescence (WDXRF) 340
20.5 Applications of XRF 344
20.6 X-Ray Diffraction (XRD) 345
21 Chromatography-Introduction and Theory 354
21.1 Preface 354
21.2 Introduction to Chromatography 354
21.3 Theory of Chromatography 354
21.4 The Theoretical Plate Number N 358
...| Erscheinungsjahr: | 2024 |
|---|---|
| Fachbereich: | Theoretische Chemie |
| Genre: | Chemie, Importe |
| Rubrik: | Naturwissenschaften & Technik |
| Medium: | Buch |
| Inhalt: | 688 S. |
| ISBN-13: | 9781119894452 |
| ISBN-10: | 111989445X |
| Sprache: | Englisch |
| Einband: | Gebunden |
| Autor: |
Ham, Bryan M
Maham, Aihui |
| Auflage: | 2nd edition |
| Hersteller: | Wiley |
| Verantwortliche Person für die EU: | Wiley-VCH GmbH, Boschstr. 12, D-69469 Weinheim, amartine@wiley-vch.de |
| Maße: | 282 x 218 x 44 mm |
| Von/Mit: | Bryan M Ham (u. a.) |
| Erscheinungsdatum: | 12.03.2024 |
| Gewicht: | 2,109 kg |
Bryan M. Ham, PhD, has worked in analytical chemistry laboratories for more than 25 years. He is currently working for the Department of Homeland Security at the U.S. Customs and Border Protection Office of Trade Headquarters in Washington D.C.
Aihui MaHam, PhD, is an expert in nano-materials including the synthesis and characterization of chemical and biological nano-sensors. She is currently working for the Department of Homeland Security at the U.S. Customs and Border Protection Office of Trade Headquarters in Washington D.C.
About the Authors xxiii
Preface xxv
Acknowledgments xxvii
About the Companion Website xxviii
1 Chemist and Technician in the Analytical Laboratory 1
1.1 Introduction-The Analytical Chemist and Technician 1
1.2 Today's Laboratory Chemist and Technician 1
1.3 ChemTech-The Chemist and Technician Toolkit Companion 2
1.4 Chapter Layout 2
1.5 Users of ChemTech 6
2 Introduction to the Analytical Laboratory 7
2.1 Introduction to the Laboratory 7
2.2 Laboratory Glassware 7
2.3 Conclusion 18
3 Laboratory Safety 19
3.1 Introduction 19
3.2 Proper Personal Protection and Appropriate Attire 19
3.3 Proper Shoes and Pants 20
3.4 Laboratory Gloves 20
3.5 General Rules to Use Gloves 22
3.6 Safety Data Sheet (SDS) 22
3.7 Emergency Eyewash and Face Wash Stations 24
3.8 Emergency Safety Showers 25
3.9 Fire Extinguishers 25
3.10 Clothing Fire in The Laboratory 26
3.11 Spill Cleanup Kits 26
3.12 Chemicals and Solvents 27
3.13 First Aid Kits 29
3.14 Gasses and Cylinders 29
3.15 Sharps Containers and Broken Glass Boxes 30
3.16 Occupational Safety and Health Administration (OSHA) 30
4 Basic Mathematics in the Laboratory 83
4.1 Introduction to Basic Math 83
4.2 Units and Metric System 83
4.3 Significant Figures 84
4.4 Scientific Calculators 86
4.5 ChemTech Conversion Tool 89
4.6 Chapter Key Concepts 96
4.7 Chapter Problems 96
5 Analytical Data Treatment (Statistics) 97
5.1 Errors in the Laboratory 97
5.2 Expressing Absolute and Relative Errors 98
5.3 Precision 98
5.4 The Normal Distribution Curve 98
5.5 Precision of Experimental Data 100
5.6 Normal Distribution Curve of a Sample 101
5.7 ChemTech Statistical Calculations 102
5.8 Student's Distribution t Test for Confidence Limits 105
5.9 Tests of Significance 111
5.10 Treatment of Data Outliers 112
5.11 Chapter Key Concepts 114
5.12 Chapter Problems 114
6 Plotting and Graphing 116
6.1 Introduction to Graphing 116
6.2 Graph Construction 116
6.3 Rectangular Cartesian Coordinate System 117
6.4 Curve Fitting 117
6.5 Redrawn Graph Example 117
6.6 Graphs of Equations 118
6.7 Least-Squares Method 121
6.8 Computer-Generated Curves 122
6.9 Calculating Concentrations 125
6.10 Nonlinear Curve Fitting 126
6.11 Chapter Key Concepts 130
6.12 Chapter Problems 130
7 Using Microsoft Excel® in the Laboratory 132
7.1 Introduction to Excel® 132
7.2 Opening Excel in ChemTech 132
7.3 The Excel Spreadsheet 132
7.4 Graphing in Excel 134
7.5 Complex Charting in Excel 137
7.6 Statistical Analysis using Excel 139
8 Making Laboratory Solutions 151
8.1 Introduction 151
8.2 Laboratory Reagent Fundamentals 151
8.3 The Periodic Table 151
8.4 Calculating Formula Weights 152
8.5 Calculating The Mole 152
8.6 Molecular Weight Calculator 152
8.7 Expressing Concentration 153
8.8 The Parts PER (PP) Notation 157
8.9 Computer-Based Solution Calculations 157
8.10 Reactions in Solution 161
8.11 Chapter Key Concepts 161
8.12 Chapter Problems 162
9 Acid-Base Theory and Buffer Solutions 163
9.1 Introduction 163
9.2 Acids and Bases in Everyday Life 163
9.3 The Litmus Test 163
9.4 Early Acid-Base Descriptions 164
9.5 Br¿nsted-Lowry Definition 164
9.6 The Equilibrium Constant 165
9.7 The Acid Ionization Constant 165
9.8 Calculating the Hydrogen Ion Concentration 165
9.9 The Base Ionization Constant 167
9.10 Ion Product for Water 168
9.11 The Solubility Product Constant (K SP) 168
9.12 The pH of a Solution 170
9.13 Measuring the pH 171
9.14 Buffered Solutions-Description and Preparing 172
9.15 ChemTech Buffer Solution Calculator 174
9.16 Chapter Key Concepts 175
9.17 Chapter Problems 175
10 Titration-A Volumetric Method of Analysis 178
10.1 Introduction 178
10.2 Reacting Ratios 178
10.3 The Equivalence Point 179
10.4 Useful Relationships for Calculations 179
10.5 Deriving the Titration Equation 179
10.6 Titrations in ChemTech 180
10.7 Acid/Base Titration Endpoint (Equivalence Point) 181
10.8 Acid/Base Titration Midpoint 182
10.9 Acid/Base Titration Indicators 182
10.10 Titrations Using Normal Solutions 184
10.11 Polyprotic Acid Titration 184
10.12 ChemTech Calculation of Normal Titrations 185
10.13 Performing a Titration 185
10.14 Primary Standards 186
10.15 Standardization of Sodium Hydroxide 187
10.16 Conductometric Titrations (Nonaqueous Solutions) 189
10.17 Precipitation Titration (MOHR Method for Halides) 190
10.18 Complex Formation with Back Titration (Volhard Method for Anions) 191
10.19 Chapter Key Concepts 196
10.20 Chapter Problems 197
11 Oxidation-Reduction (Redox) Reactions 199
11.1 Introduction 199
11.2 Oxidation and Reduction 199
11.3 The Volt 200
11.4 The Electrochemical Cell 200
11.5 Redox Reaction Conventions 200
11.6 The Nernst Equation 202
11.7 Determining Redox Titration Endpoints 203
11.8 Potentiometric Titrations 204
11.9 Visual Indicators used in Redox Titrations 206
11.10 Pretitration Oxidation-Reduction 207
11.11 Ion-Selective Electrodes 207
11.12 Chapter Key Concepts 207
11.13 Chapter Problems 209
12 Laboratory Information Management System (LIMS) 211
12.1 Introduction 211
12.2 Lims Main Menu 211
12.3 Logging in Samples 213
12.4 Entering Test Results 213
12.5 Add or Delete Tests 214
12.6 Calculations and Curves 214
12.7 Search Wizards 215
12.8 Approving Samples 217
12.9 Printing Sample Reports 217
13 Ultraviolet and Visible (UV/VIS) Spectroscopy 227
13.1 Introduction to Spectroscopy in the Analytical Laboratory 227
13.2 The Electromagnetic Spectrum 227
13.3 Ultraviolet/Visible (UV/VIS) Spectroscopy 227
13.4 UV/Visible Spectrophotometers 236
13.5 Special Topic (Example)-Spectrophotometric Study of Dye Compounds 237
13.6 Chapter Key Concepts 240
13.7 Chapter Problems 242
14 Fluorescence Optical Emission Spectroscopy 244
14.1 Introduction to Fluorescence 244
14.2 Fluorescence and Phosphorescence Theory 245
14.3 Phosphorescence 246
14.4 Excitation and Emission Spectra 247
14.5 Rate Constants 247
14.6 Quantum Yield Rate Constants 248
14.7 Decay Lifetimes 248
14.8 Factors Affecting Fluorescence 249
14.9 Quantitative Analysis and Beer-Lambert Law 252
14.10 Quenching of Fluorescence 253
14.11 Fluorometric Instrumentation 253
14.12 Special Topic-Fluorescence Study of Dye-A007 Complexes 259
14.13 Chapter Key Concepts 261
14.14 Chapter Problems 262
15 Fourier Transform Infrared (FTIR) Spectroscopy 264
15.1 Introduction 264
15.2 Basic IR Instrument Design 264
15.3 The Infrared Spectrum and Molecular Assignment 266
15.4 FTIR Table Band Assignments 267
15.5 FTIR Spectrum Example I 273
15.6 FTIR Spectrum Example II 273
15.7 FTIR Inorganic Compound Analysis 274
15.8 Chapter Key Concepts 274
15.9 Chapter Problems 276
16 Nuclear Magnetic Resonance (NMR) Spectroscopy 280
16.1 Introduction 280
16.2 Frequency and Magnetic Field Strength 280
16.3 Continuous-Wave NMR 281
16.4 The NMR Sample Probe 282
16.5 Pulsed-Field Fourier Transform NMR 282
16.6 Proton NMR Spectra Environmental Effects 284
16.7 Carbon-13 NMR 286
16.8 Special Topic-NMR Characterization of Cholesteryl Phosphate 290
16.9 Chapter Key Concepts 295
16.10 Chapter Problems 296
References 297
17 Atomic Absorption Spectroscopy (AAS) 298
17.1 Introduction 298
17.2 Atomic Absorption and Emission Process 298
17.3 Atomic Absorption and Emission Source 299
17.4 Source Gases and Flames 299
17.5 Block Diagram of AAS Instrumentation 299
17.6 The Light Source 301
17.7 Interferences in AAS 302
17.8 Electrothermal Atomization-Graphite Furnace 302
17.9 Instrumentation 303
17.10 Flame Atomic Absorption Analytical Methods 304
18 Atomic Emission Spectroscopy 306
18.1 Introduction 306
18.2 Elements in Periodic Table 306
18.3 The Plasma Torch 306
18.4 Sample Types 307
18.5 Sample Introduction 308
18.6 ICP-OES Instrumentation 308
18.7 ICP-OES Environmental Application Example 313
19 Atomic Mass Spectrometry 328
19.1 Introduction 328
19.2 Low-Resolution ICP-MS 328
19.3 High-Resolution ICP-MS 331
20 X-Ray Fluorescence (XRF) and X-Ray Diffraction (XRD) 336
20.1 X-Ray Fluorescence Introduction 336
20.2 X-Ray Fluorescence Theory 336
20.3 Energy-Dispersive X-Ray Fluorescence (EDXRF) 337
20.4 Wavelength Dispersive X-Ray Fluorescence (WDXRF) 340
20.5 Applications of XRF 344
20.6 X-Ray Diffraction (XRD) 345
21 Chromatography-Introduction and Theory 354
21.1 Preface 354
21.2 Introduction to Chromatography 354
21.3 Theory of Chromatography 354
21.4 The Theoretical Plate Number N 358
...| Erscheinungsjahr: | 2024 |
|---|---|
| Fachbereich: | Theoretische Chemie |
| Genre: | Chemie, Importe |
| Rubrik: | Naturwissenschaften & Technik |
| Medium: | Buch |
| Inhalt: | 688 S. |
| ISBN-13: | 9781119894452 |
| ISBN-10: | 111989445X |
| Sprache: | Englisch |
| Einband: | Gebunden |
| Autor: |
Ham, Bryan M
Maham, Aihui |
| Auflage: | 2nd edition |
| Hersteller: | Wiley |
| Verantwortliche Person für die EU: | Wiley-VCH GmbH, Boschstr. 12, D-69469 Weinheim, amartine@wiley-vch.de |
| Maße: | 282 x 218 x 44 mm |
| Von/Mit: | Bryan M Ham (u. a.) |
| Erscheinungsdatum: | 12.03.2024 |
| Gewicht: | 2,109 kg |
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